Extracurricular laboratory: Synthetic route of 14024-18-1

As the rapid development of chemical substances, we look forward to future research findings about 14024-18-1

Iron(III) acetylacetonate, cas is 14024-18-1, it is a common heterocyclic compound, the iron-catalyst compound, its synthesis route is as follows.,14024-18-1

Nanoparticles narrow diameter distribution were prepared by the high-temperature decompositionof Co(acac)2 and Fe(acac)3 with the 1:2 Mratio (0.6:1.2mmol) together with 1-2 octanediol, diphenyl ether (boiling point at 550 K)and oleic acid and oley-lamina as surfactants. The particle size was tailored by the sur-factant: precursor molar ratio ([Surf.]:[Prec.])according to there-ference [15]. The preparation was magnetically stirred and heated up to the boiling temperature T535 K for 120 min. After synthesis the nanoparticles were extracted by adding ethanol followed by centrifugation(14,000rpm/30min). After that,they were washed with acetone and centrifuged once again. The final sample consists in a black powder constituted by cobalt ferrite nanoparticles covered with an oleic acid layer, which is strongly linked to the surface, improving the chemical stability, and avoiding agglomeration. The samples were labeled S2,S5,and S7 with mean diameter 2.0,4.5,and 7.0 nm respectively, obtained from the TEM analysis.

As the rapid development of chemical substances, we look forward to future research findings about 14024-18-1

Reference£º
Article; Pianciola, Betiana N.; Lima, Enio; Troiani, Horacio E.; Nagamine, Luiz C.C.M.; Cohen; Zysler, Roberto D.; Journal of Magnetism and Magnetic Materials; vol. 377; (2015); p. 44 – 51;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion