1273-86-5, Ferrocenemethanol is a iron-catalyst compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Under a nitrogen atmosphere, 4-aminobenzenesulfonamide (172 mg, 1 mmol)[Cp * IrCl2] 2 (8 mg, 0.01 mmol, 1 mol%),Cesium carbonate (65 mg, 0.2 mmol),Ferrocene methanol (259 mg, 1.2 mmol)Tert-amyl alcohol (1.0 mL) was added sequentially to a 25 mL Schlenk reaction flask.The mixture was allowed to react at 120 C for 12 hours,Cooled to room temperature,The solvent was removed under vacuum.And then passed through a column chromatography (developing solvent: ethyl acetate / n-hexane)To pure target compound, yield: 80%.
1273-86-5, The synthetic route of 1273-86-5 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; NANJING UNIVERSITY OF SCIENCE AND TECHNOLOGY; LI, FENG; LU, LEI; MA, JUAN; (16 pag.)CN106146358; (2016); A;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion