14024-18-1, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. Iron(III) acetylacetonate, cas is 14024-18-1,the iron-catalyst compound, it is a common compound, a new synthetic route is introduced below.
Fe(acac)3 (3?mmol, 0.706?g) was dissolved in oleylamine (15?mL) and benzyl ether (15?mL) mixed solution and magnetically stirred under a flow of nitrogen. The mixture was dehydrated at 110?C for 1?h, then quickly heated to 300?C at a heating rate of 20?C/min and allowed to react for another 1?h. The black-brown mixture was cooled to room temperature and extract with ethanol (40?mL) to precipitate out the crude Fe3O4 MNPs, which was collected by centrifugation (8000?rpm, 10?min). The black product was then purified by dissolving in hexane (35?mL) and reprecipitating by addition of ethanol (50?mL) for 3 times to give rise to pure Fe3O4 MNPs in black powder (0.15?g). hydrophobic to hydrophilic.
The chemical industry reduces the impact on the environment during synthesis,14024-18-1,Iron(III) acetylacetonate,I believe this compound will play a more active role in future production and life.
Reference£º
Article; Guo, Hongen; Zhang, Yixia; Liang, Wenting; Tai, Feifei; Dong, Qingchen; Zhang, Ruiping; Yu, Baofeng; Wong, Wai-Yeung; Journal of Inorganic Biochemistry; vol. 192; (2019); p. 72 – 81;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
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