1273-86-5, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. Ferrocenemethanol, cas is 1273-86-5,the iron-catalyst compound, it is a common compound, a new synthetic route is introduced below.
Ferrocenemethanol (1.3 mmol), 4-methylaniline (1 mmol), carbon-supported ruthenium nanomaterial (20 mg),Potassium hydroxide (20 mg) was added to a 25 ml reaction tube with a magnetic stirrer.After repeated nitrogen suction three times, toluene (3 ml) was added via a syringe and then sealed and reacted at 110C for 24 hours.After the reaction is completed, the catalyst is removed by filtration, and the filtrate is extracted by adding water and ethyl acetate, and the organic phases are combined.After drying, filtration, concentration under reduced pressure, and silica gel column chromatography, N-(ferrocenyl)aniline (yield 85%) was obtained.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of Ferrocenemethanol, 1273-86-5
Reference£º
Patent; Soochow University (Suzhou); Li Hongxi; Guo Bin; Lang Jianping; (16 pag.)CN107954879; (2018); A;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion