Downstream synthetic route of Acetylferrocene

1271-55-2, In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles.,1271-55-2 ,Acetylferrocene, other downstream synthetic routes, hurry up and to see

As a common heterocyclic compound, it belongs to iron-catalyst compound, name is Acetylferrocene, and cas is 1271-55-2, its synthesis route is as follows.

To a 100 mL round bottom reaction flask was added p-toluenesulfonyl hydrazide (1.5 eq)Methanol was gradually added until the p-toluenesulfonyl hydrazide was completely dissolved.Heated to 60oC,After a small amount of methanol was used to dissolve acetyl ferrocene (1 equivalent) prepared in the previous reaction,Was added dropwise to p-toluenesulfonyl hydrazide solution,Stirring to reflux to a large amount of solid precipitation.Suction filtered, washed with petroleum ether,Dry, getAcetylferrocene p-toluenesulfonyl hydrazone.Yield 81%.

1271-55-2, In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles.,1271-55-2 ,Acetylferrocene, other downstream synthetic routes, hurry up and to see

Reference：
Patent; Inner Mongolia University; Zhang Hao; Ling Li; Hu Jianfeng; Huo Yanhong; (11 pag.)CN107226829; (2017); A;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
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