102-54-5, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. Ferrocene, cas is 102-54-5,the iron-catalyst compound, it is a common compound, a new synthetic route is introduced below.
Ferrocene (0.500 g, 2.69 mmol) and acetic anhydride (1.7 mL) were dissolved in acid, phosphoric acid aqueous solution (85% in 0 oC, 0.53 g, were placed 0.30 mL, 4.8 mmol). After heating the reaction mixture under reflux for 15 minutes, it poured into a beaker containing 20 g of ice. After all the ice is melted were placed in a saturated aqueous solution of sodium bicarbonate until air bubbles are no longer generated. The reaction mixture was cooled to 0 dried under reduced pressure gave filtered while washing the resulting solid with water to give a red solid Compound 1b. (0.598 g, 97%).
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of Ferrocene, 102-54-5
Reference:
Patent; Diatech Korea Co. Ltd.; Sogang University Research Foundation; Moon, PongJin; Oh, HaNa; Kang, NaNa; Cheon, AeRan; Park, Gye Shin; Park, Hyeong Soon; Pang, Choo Young; (31 pag.)KR101583811; (2016); B1;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
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