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An alternative method for the preparation of 1-ferrocenylalkyl alcohols has been developed.This involves condensation of ferrocene with carbonyl compounds in concentrated sulfuric acid and addition of the resulting solutions of 1-ferrocenylalkylium ions into aqueous sodium bicarbonate.The mixtures are then treated with thioglycolic acid and the S-(1-ferrocenylalkyl)thioglycolic acids purified via sodium salts and hydrolysed in the presence of copper powder to give 1-ferrocenylalkyl alcohols in good yields.
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Reference：
Iron Catalysis in Organic Synthesis | Chemical Reviews,
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion