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A systematic study of the reactions of a number of alpha-hydroxylated ferrocene derivatives with thioglycolic acid confirms that the reaction is extremely fast, viz., 15-20 min <1>, as compared with earlier procedures (12 h) <2,3>.The important kinetic parameters of the reaction of 1-ferrocenylethanol with the thioglycolic acid in the presence of trifluoroacetic acid have been determined.
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Reference：
Iron Catalysis in Organic Synthesis | Chemical Reviews,
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion