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Moessbauer and NMR spectra are reported for ferrocenyl (Fc) carbenium ions, FcCH2+ (III+) and FcC+Me2 (II+) in frozen acidic media. 1H-NMR spectra showed no evidence of Fe-H bonded species.Moessbauer parameters for II+ were identical within experimental error to those obtained for the carbenium ion precursors and to ferrocene itself, whereas quadrupole splittings for III+ were significantly larger.The results for the latter species are interpreted in terms of stabilisation via orbital overlaps with the central iron atom.
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Reference：
Iron Catalysis in Organic Synthesis | Chemical Reviews,
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion