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The sol-gel polycondensation of tetramethoxysilane has been followed for the first time by functionalization of the oligomeric silane species with a redox active ferrocene. Recording the decrease of the average diffusion coefficient of the mobile species brings information on the sol or gel state, as well as an easy insight of the polycondensation kinetics.
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Reference：
Iron Catalysis in Organic Synthesis | Chemical Reviews,
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion