The iron-catalyst compound, cas is 1273-86-5 name is Ferrocenemethanol, mainly used in chemical industry, its synthesis route is as follows.,1273-86-5
Acetophenone (60 mg, 0.5 mmol),Cat. [Ir] (5.4 mg, 0.005 mmol, 1.0 mol%),Cesium carbonate (33 mg, 0.1 mmol, 0.2 equiv.),Ferrocene methanol (130 mg, 0.6 mmol)And tert-amyl alcohol (1 ml) were successively added to a 5 mL round bottom flask.The reaction mixture was refluxed in air for 12 hours,Cool to room temperature.Rotate the solvent to remove the solvent,The purified title compound was then purified by column chromatography (developing solvent: petroleum ether / ethyl acetate)Yield: 92%
With the rapid development of chemical substances, we look forward to future research findings about 1273-86-5
Reference£º
Patent; Nanjing University of Science and Technology; Liu, Pengcheng; Lu, Lei; Li, Feng; (12 pag.)CN106478395; (2017); A;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion