Iron(III) acetylacetonate, cas is 14024-18-1, it is a common heterocyclic compound, the iron-catalyst compound, its synthesis route is as follows.,14024-18-1
Synthesis of ferrimagnetic nanocubes ( Fe3O4 ) was carried out under nitrogen (N 2).Typical synthesis of mangnetic nanocubes ( 0.71g,2 mmol ) Iron ( III ) acetylacetonate (Fe(acac)3) mixed with ( 0.41 g,2.1 mmol ) 4-biphenylacarboxylic acid added to mixture ( 1.129 g , 4 mmol ) oleic acid and ( 10.40 g ,10 ml ) benzyl ether . The mixture solution was degassed at room temperature for 1 hour .The solution was then heated to 290C at the rate of 20C /min with vigorous magnetic stirring at 290 rpm to get ferrimagnetic nanocubes. where the temperature was held for 30 min when temperature reached 290C . After cooling the solution to room temperature , a mixture of ( 40 ml ) toluene and ( 10 ml ) hexane was added to solution . The solution was then centrifuged at 5000 rpm for minutes to precipitate the magnetite nanocubes .The precipitate was washed using ( 10 ml ) chloroform ( CHCl3 ) . Then after that used oven vacuum to obtain Fe3O4 nanocubes in powder form at 80C temperature14- 18.
14024-18-1 is used more and more widely, we look forward to future research findings about Iron(III) acetylacetonate
Reference£º
Article; Alkadasi, Nabil Abdullah Noman; Oriental Journal of Chemistry; vol. 30; 3; (2014); p. 1179 – 1182;,
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