As a common heterocyclic compound, it belong iron-catalyst compound,Ferrocenecarboxylic acid,1271-42-7,Molecular formula: C11H10FeO2,mainly used in chemical industry, its synthesis route is as follows.,1271-42-7
Oxalyl chloride (0.058 mL, 0.66 mmol) was added dropwise over 1 min to a solution of ferrocene monocarboxylic acid (0.0777 g, 0.338 mmol) in dichloromethane (3.0 mL) and N,N-dimethylformamide (1-3 drops). The mixture stirred for 30 min and concentrated with a stream of nitrogen gas, and then subjected to vacuum for 10 min. The resultant crude oil was used without further purification.
With the synthetic route has been constantly updated, we look forward to future research findings about Ferrocenecarboxylic acid,belong iron-catalyst compound
Reference£º
Article; Jones, Ian M.; Knipe, Peter C.; Michaelos, Thoe; Thompson, Sam; Hamilton, Andrew D.; Molecules; vol. 19; 8; (2014); p. 11316 – 11332;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion