1271-51-8, Vinylferrocene is a iron-catalyst compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
General procedure: 25mL reaction flask, weighing 2molpercent palladium acetate and 4molpercent ferrocenylpyrimidine multidentate ligand 6h, adding 12 water, stirring for 5min, 4 mmol of p-nitrochlorobenzene, 4.8 mmol of butyl acrylate, 6 mmol of potassium phosphate, and 0.8 mmol of tetrabutylammonium bromide were added successively. The reaction was heated to 80¡ãC until the reaction was complete (the reaction did not continue after about 6 h, and palladium black appeared in the reaction flask). After adding 25 mL of ethyl acetate and washing three times with water, the organic phases were combined, dried over anhydrous sodium sulfate, concentrated, and the residue was separated by column chromatography. PE/EA=12:1 was used as an eluent to obtain 707 mg of a yellow solid with a yield of 71percent.
1271-51-8, 1271-51-8 Vinylferrocene 16211828, airon-catalyst compound, is more and more widely used in various fields.
Reference£º
Patent; Zhengzhou University of Light Industry; Yu Shuyan; Zhang Tongyan; Wang Ruijuan; Yin Zhigang; Yang Xuzhao; Lan Hongbing; (13 pag.)CN107383112; (2017); A;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion