14024-18-1, Iron(III) acetylacetonate is a iron-catalyst compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Fe3O4 nanoparticles were prepared by the following synthetic procedure, which was based on our previous study [29]: the reaction was carried out in the 100 mL three-necked round-bottom flask equipped with a condenser and a thermometer. The heating was carried out by a heating mantle. Iron acetylacetonate (III) (1 mmol) and 1,2-hexadecanediol (3.0 mmol) as Fe3+ reducing agent were added into a mixture of oleic acid (15 mmol) and distilled oleylamine (15 mmol). The solution was maintained at 130 C for 30 min with vigorous stirring under a reduced atmosphere (ca. 200 Pa) for dissolution and removal of impurities such as water molecules and organic molecules with low boiling temperatures. In this phase, the solution color was dark brown. Then, the solution was heated to reaction temperatures of 200 C, 250 C, 280 C, and 300 C for 1 h, 3 h, and 6 h under a nitrogen atmosphere (1 atm.). The solution color changed to black. Finally, the solution was left to cool to room temperature by remove of the heat source. When the solution becomes hard or loses fluidity after cooling to room temperature, the resulting solidified solution was dissolved by adding 10 mL n-hexane before the following precipitation process. The iron oxide nanoparticles were precipitated by the addition of ethanol (70~80 mL) and were subsequently subjected to centrifugation (3000 g, 10 min).The precipitated nanoparticles were redispersed into n-hexane., 14024-18-1
14024-18-1 Iron(III) acetylacetonate 91759530, airon-catalyst compound, is more and more widely used in various fields.
Reference£º
Article; Nakaya, Masafumi; Nishida, Ryo; Muramatsu, Atsushi; Molecules; vol. 19; 8; (2014); p. 11395 – 11403;,
Iron Catalysis in Organic Synthesis | Chemical Reviews
Iron Catalysis in Organic Synthesis: A Critical Assessment of What It Takes To Make This Base Metal a Multitasking Champion